1: With n-butyllithium; zirconocene dichloride in tetrahydrofuran; hexane T=-78 - 20°C; 2: With iodine in tetrahydrofuran; hexane T=-20 - 20°C; Further stages.;
参考文献
Farhat, Shahera; Zouev, Irena; Marek, Ilan
Tetrahedron, 2004 , vol. 60, # 6 p. 1329 - 1337
Wolff, Russell R.; Basava, Vikram; Giuliano, Robert M.; Boyko, Walter J.; Schauble, J. Herman
Canadian Journal of Chemistry, 2006 , vol. 84, # 4 p. 667 - 675
1: 86 percent / N-iodosuccinimide / CH2Cl2 / 20 °C
2: 95 percent / neutral alumina / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Wolff, Russell R.; Basava, Vikram; Giuliano, Robert M.; Boyko, Walter J.; Schauble, J. Herman
Canadian Journal of Chemistry, 2006 , vol. 84, # 4 p. 667 - 675
Finikova, Olga S.; Cheprakov, Andrei V.; Beletskaya, Irina P.; Carroll, Patrick J.; Vinogradov, Sergei A.
Journal of Organic Chemistry, 2004 , vol. 69, # 2 p. 522 - 535
