4'-(壬氧基)[1,1'-联苯]-4-甲腈合成路线 (共 7 条)
反应条件
(Ph3P)2Pd(Ph)(I) in N,N-dimethyl-formamide
2 h; Heating;
参考文献
Bumagin, N. A.; Luzikova, E. V.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1480 - 1486
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1650 - 1656
反应条件
sodium isopropanolate in isopropyl alcohol
1 h; Heating;
参考文献
Ruolene, Yu. I.; Adomenas, P. V.; Adomenene, O. K.; Denis, G. I.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1192 - 1195
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1310 - 1314
反应条件
1: 70 percent / SnCl2, conc.HCl / propan-2-ol / 0.17 h / Heating
2: NaNO2, 10percent aq. H2SO4 / acetic acid / Heating
3: 56 percent / sodium isopropoxide / propan-2-ol / 1 h / Heating
View Scheme
参考文献
Ruolene, Yu. I.; Adomenas, P. V.; Adomenene, O. K.; Denis, G. I.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1192 - 1195
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1310 - 1314
反应条件
1: NaNO2, 10percent aq. H2SO4 / acetic acid / Heating
2: 56 percent / sodium isopropoxide / propan-2-ol / 1 h / Heating
View Scheme
参考文献
Ruolene, Yu. I.; Adomenas, P. V.; Adomenene, O. K.; Denis, G. I.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1192 - 1195
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1310 - 1314
反应条件
1: 20percent KOH / propan-2-ol / Heating
2: 56 percent / sodium isopropoxide / propan-2-ol / 1 h / Heating
View Scheme
参考文献
Ruolene, Yu. I.; Adomenas, P. V.; Adomenene, O. K.; Denis, G. I.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1192 - 1195
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1310 - 1314
反应条件
1: PdCl2(dppf) / tetrahydrofuran / 0.25 h / 20 °C
2: 86 percent / PhPdI(PPh3)2 / dimethylformamide / 2 h / Heating
View Scheme
参考文献
Bumagin, N. A.; Luzikova, E. V.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1480 - 1486
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1650 - 1656
反应条件
1-methyl-pyrrolidin-2-one
参考文献
Gray,G.W.; Mosley,A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1976 , p. 97 - 102