in neat (no solvent) heating to 50°C in vacuum; after 30min;;
参考文献
Tajiri; Matsumoto; Deguchi; Mito; Takagi; Moriyoshi; Itoh; Koyama
Journal of Magnetism and Magnetic Materials, 2007 , vol. 310, # 2 SUPPL. PART 2 p. e566-e568
in neat (no solvent) heating to 50°C in vacuum; after 30min;;
参考文献
Tajiri; Matsumoto; Deguchi; Mito; Takagi; Moriyoshi; Itoh; Koyama
Journal of Magnetism and Magnetic Materials, 2007 , vol. 310, # 2 SUPPL. PART 2 p. e566-e568
water in water
byproducts: H2, CO2; High Pressure; soln. of Cu salt heated in Ti alloy reactor under N2 atm. to 673 K at 30MPa for 5 min, kept at this temp. for 30 min; reactor quenched in water bath; XRD;