乙基3-(3-甲氧基苯基)-2-丙炔酸酯合成路线 (共 4 条)
反应条件
caesium carbonate; triphenylphosphine; silver(l) oxide in dichloromethane
T=35°C; 3 h; Inert atmosphere;
参考文献
Nie, Xiaopeng; Liu, Suli; Zong, Yan; Sun, Peipei; Bao, Jianchun
Journal of Organometallic Chemistry, 2011 , vol. 696, # 8 p. 1570 - 1573
反应条件
copper(l) iodide; cesium fluoride in toluene; acetonitrile
T=150°C; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Akubathini, Shashidhar Kumar; Biehl, Ed
Tetrahedron Letters, 2009 , vol. 50, # 16 p. 1809 - 1811
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in tetrahydrofuran
T=80°C; 0.0833333 h; Inert atmosphere;
2: With copper(l) iodide in tetrahydrofuran
T=65°C; 8 h; Inert atmosphere;
参考文献
Cai, Shunyou; Yang, Kai; Wang, David Zhigang
Organic Letters, 2014 , vol. 16, # 10 p. 2606 - 2609
反应条件
1: (3-methoxy-phenyl)-acetylene With n-butyllithium
2: chloroformic acid ethyl ester
参考文献
Durham, Robin; Mandel, Jeremie; Blanchard, Nicolas; Tam, William
Canadian Journal of Chemistry, 2011 , vol. 89, # 12 p. 1494 - 1505