乙基3-(3-甲基苯基)-2-丙炔酸酯合成路线 (共 2 条)
反应条件
copper(l) iodide; air; caesium carbonate; silver(l) oxide in dichloromethane
T=80°C; Sonogashira type reaction; 36 h;
参考文献
Pan, Changduo; Luo, Fang; Wang, Wenhui; Ye, Zhishi; Cheng, Jiang
Tetrahedron Letters, 2009 , vol. 50, # 35 p. 5044 - 5046
反应条件
1: 1-ethynyl-3-methylbenzene With n-butyllithium
2: chloroformic acid ethyl ester
参考文献
Durham, Robin; Mandel, Jeremie; Blanchard, Nicolas; Tam, William
Canadian Journal of Chemistry, 2011 , vol. 89, # 12 p. 1494 - 1505