2-(叔丁基)-3,3-二甲基-1-丁烯合成路线 (共 32 条)
参考文献
Nasarow
Chemische Berichte, 1936 , vol. 69, p. 20
Doklady Akademii Nauk SSSR, 1936 , vol. 10, p. 81
Chem. Zentralbl., 1936 , vol. 107, # II p. 59
参考文献
Nasarow
Chemische Berichte, 1936 , vol. 69, p. 20
Doklady Akademii Nauk SSSR, 1936 , vol. 10, p. 81
Chem. Zentralbl., 1936 , vol. 107, # II p. 59
反应条件
1: 1) BH3*THF; 2) 30percent aq. H2O2, NaOH / 1) r.t., 4 h; 2) EtOH, r.t., 1 h 2: 85 percent / CrO3, aq. H2SO4 / acetone / 4 h / Ambient temperature; ultrasound sonication 3: 86 percent / SOCl2 / 1 h / 60 - 65 °C View Scheme
参考文献
Newman,M.S. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 2498 - 2501
反应条件
ozone in diethyl ether T=-70°C;
参考文献
Kawamura, Shin-Ichi; Yamakoshi, Hideyuki; Abe, Manabu; Masuyama, Araki; Nojima, Masatomo
Tetrahedron, 2002 , vol. 58, # 5 p. 891 - 896
参考文献
Howard et al.
Journal of Research of the National Bureau of Standards (United States), 1947 , vol. 38, p. 391
Chem. Zentralbl., 1947 , vol. 118, p. 5291
Full Text Show Details
Whitmore; Laughlin
Journal of the American Chemical Society, 1933 , vol. 55, p. 3736
参考文献
Nasarow
Chemische Berichte, 1936 , vol. 69, p. 20
Doklady Akademii Nauk SSSR, 1936 , vol. 10, p. 81
Chem. Zentralbl., 1936 , vol. 107, # II p. 59
反应条件
nickel kieselguhr Hydrogenation.unter Druck;
参考文献
Journal of Research of the National Bureau of Standards (United States), vol. 38, p. 384,390
Chem.Abstr., , p. 5291
反应条件
64 h; Irradiationother solvents; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 103, # 24 p. 7293 - 7298
反应条件
thionyl chloride in pyridine
T=0 - 5°C;
参考文献
Dubois, Jacques-Emile; Zhang, Ben Li; Lion, Claude
Tetrahedron, 1981 , vol. 37, # 24 p. 4189 - 4194
反应条件
1: 91 percent / diethyl ether / 1 h / Heating
2: 91 percent / SOCl2 / pyridine / 0 - 5 °C
View Scheme
参考文献
Dubois, Jacques-Emile; Zhang, Ben Li; Lion, Claude
Tetrahedron, 1981 , vol. 37, # 24 p. 4189 - 4194