3-异丙氧基环己-2-烯-1-酮合成路线 （共 7 条）
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile 2.5 h; Heating;
参考文献
Banerjee, Biplab; Mandal, Samir Kumar; Roy, Subhas Chandra
Chemistry Letters, 2006 , vol. 35, # 1 p. 16 - 17
反应条件
ytterbium(III) triflate
T=20°C; 12 h;
参考文献
Curini, Massimo; Epifano, Francesco; Genovese, Salvatore
Tetrahedron Letters, 2006 , vol. 47, # 27 p. 4697 - 4700
反应条件
1: hex-5-ynoic acid With oxalyl dichloride in dichloromethane
2.5 h; Inert atmosphere;
2: With indium(III) chloride in dichloromethane
3 h; Inert atmosphere;
3: isopropyl alcohol in dichloromethane
T=90°C; 0.25 h; Inert atmosphere;
参考文献
Hylden, Anne T.; Uzelac, Eric J.; Ostojic, Zeljko; Wu, Ting-Ting; Sacry, Keely L.; Sacry, Krista L.; Xi, Lin; Jones, T. Nicholas
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1323 - 1326
反应条件
magnesium; diisopropylamine in tetrahydrofuran; dichloromethane; ethyl acetate
参考文献
John Wyeth and Brother Limited
Patent: US4197241 A1, 1980 ;
反应条件
lithium diisopropyl amide
LHMDS, THF, HMPT; Yield given. Multistep reaction;
参考文献
Dieter, R. Karl
Journal of Organic Chemistry, 1981 , vol. 46, # 24 p. 5031 - 5033
反应条件
in tetrahydrofuran; diethyl ether
T=-78°C; 0.166667 h;
参考文献
Barriault, Louis; Thomas, Jermaine D. O.; Clement, Roxanne
Journal of Organic Chemistry, 2003 , vol. 68, # 6 p. 2317 - 2323
反应条件
in tetrahydrofuran; diethyl ether
T=-78°C; 0.166667 h;
参考文献
Barriault, Louis; Thomas, Jermaine D. O.; Clement, Roxanne
Journal of Organic Chemistry, 2003 , vol. 68, # 6 p. 2317 - 2323
