2-(二异丙基氨基)-乙烷硫醇合成路线 （共 8 条）
反应条件
in chlorobenzene Heating;
参考文献
Atkinson; Russ; Tucker
Journal of medicinal chemistry, 1971 , vol. 14, # 10 p. 1005 - 1007
反应条件
in chlorobenzene Heating;
参考文献
Atkinson; Russ; Tucker
Journal of medicinal chemistry, 1971 , vol. 14, # 10 p. 1005 - 1007
反应条件
sodium hydroxide; thiourea in water
5 h;
参考文献
Davis, Franklin A.; Ray, Jayanta K.; Kasperowicz, Steve; Przeslawski, Robert M.; Durst, H. Dupont
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2594 - 2599
反应条件
1: 2'-diisopropylaminoethyl disulfide hydrochloride With sulfuryl dichloride in dichloromethane
T=-15°C; sulfurylation; 0.333333 h;
2: (2-diisopropylaminoethylthio)ethanethiol in dichloromethane
T=20°C; Condensation;
参考文献
Rohrbaugh; Berg; Szafraniec; Rossman; Durst; Munavalli
Phosphorus, Sulfur and Silicon and Related Elements, 1999 , vol. 149, p. 95 - 106
反应条件
in acetonitrile
T=25°C; pH=8.5; Tris/HCl buffer;
参考文献
Saint-Andre, Geraldine; Kliachyna, Maria; Kodepelly, Sanjeevarao; Louise-Leriche, Ludivine; Gillon, Emilie; Renard, Pierre-Yves; Nachon, Florian; Baati, Rachid; Wagner, Alain
Tetrahedron, 2011 , vol. 67, # 34 p. 6352 - 6361
参考文献
Ratschinskii et al.
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 2998,3001,3002;engl.Ausg.S.3027,3028,3030
反应条件
water
1080 h; Ambient temperaturevarious V-type agents under different reaction conditions; Product distributionMechanism;
参考文献
Yang, Yu-Chu; Szafraniec, Linda L.; Beaudry, William T.; Rohrbaugh, Dennis K.; Procell, Lawrence R.; Samuel, John B.
Journal of Organic Chemistry, 1996 , vol. 61, # 24 p. 8407 - 8413
反应条件
sodium hydroxide; potassium iodide in water
2 h;
参考文献
Davis, Franklin A.; Ray, Jayanta K.; Kasperowicz, Steve; Przeslawski, Robert M.; Durst, H. Dupont
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2594 - 2599
