N,N-二甲基氢化肉桂酰胺合成路线 （共 32 条）
反应条件
tert-butyl alcohol in tetrahydrofuran electrolysis (Mg electrodes, LiClO4);
参考文献
Shono, Tatsuya; Masuda, Haruhisa; Murase, Hiroaki; Shimomura, Masatoshi; Kashimura, Shigenori
Journal of Organic Chemistry, 1992 , vol. 57, # 4 p. 1061 - 1063
反应条件
tert-butyl alcohol in tetrahydrofuran electrolysis (Mg electrodes, LiClO4);
参考文献
Journal of Organic Chemistry, , vol. 57, # 4 p. 1061 - 1063
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78 - -40°C; Inert atmosphere; 2: With ammonia; iodine in tetrahydrofuran; hexane; water T=0 - 20°C; Inert atmosphere;
参考文献
Suzuki, Yusuke; Yoshino, Takumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 21 p. 3809 - 3814
反应条件
pyridine; trifluoromethylsulfonic anhydride 1.) CH2Cl2, -40 to 0 deg C, 2 h; 0 deg C, 10 h, 2.) r.t., 12 h; Yield given. Multistep reaction;
参考文献
Charette, Andre B.; Chua, Peter
Synlett, 1998 , # 2 p. 163 - 165
反应条件
cerium(III) chloride; methyllithium in tetrahydrofuran T=-78°C; 0.25 h; Yield given. Yields of byproduct given;
参考文献
Kurosu, Michio; Kishi, Yoshito
Tetrahedron Letters, 1998 , vol. 39, # 27 p. 4793 - 4796
反应条件
pentacarbonyliron(0); 1,1,3,3-tetramethyldisiloxane in toluene T=20°C; Inert atmosphereIrradiation;
参考文献
Sunada, Yusuke; Kawakami, Hiroko; Imaoka, Tsuyoshi; Motoyama, Yukihiro; Nagashima, Hideo
Angewandte Chemie - International Edition, 2009 , vol. 48, # 50 p. 9511 - 9514
反应条件
polymethylhydrosiloxane; dihydrogen hexachloroplatinate in tetrahydrofuran T=90°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 47, # 35 p. 6173 - 6177
反应条件
triethylamine in diethyl ether
参考文献
Hanada, Shiori; Tsutsumi, Emi; Motoyama, Yukihiro; Nagashima, Hideo
Journal of the American Chemical Society, 2009 , vol. 131, # 41 p. 15032 - 15040
Title/Abstract Full Text View citing articles Show Details
Sunada, Yusuke; Kawakami, Hiroko; Imaoka, Tsuyoshi; Motoyama, Yukihiro; Nagashima, Hideo
Angewandte Chemie - International Edition, 2009 , vol. 48, # 50 p. 9511 - 9514
反应条件
1: styrene With 9-borabicyclo[3.3.1]nonane dimer in tetrahydrofuran
T=20°C;
2: N,N-dimethylcarbamoyl chloride With caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
16 h; Heating; Further stages.;
参考文献
Yasui, Yoshizumi; Tsuchida, Sayo; Miyabe, Hideto; Takemoto, Yoshiji
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5898 - 5900
反应条件
Fe3O4Rh; hydrazine hydrate in ethanol
T=80°C; 14 h; Inert atmosphere;
参考文献
Jang, Youngjin; Kim, Seyoung; Jun, Samuel Woojoo; Kim, Byung Hyo; Hwang, Sunhwan; Song, In Kyu; Kim, B. Moon; Hyeon, Taeghwan
Chemical Communications, 2011 , vol. 47, # 12 p. 3601 - 3603
