1-苯基-1,4-戊二酮合成路线 (共 177 条)
反应条件
triphenylphosphine; rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate in methanol T=80°C; P=15001.2 Torr; 18 h;
参考文献
Tetrahedron, , vol. 62, # 50 p. 11740 - 11746
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=100°C; 30 h;
参考文献
Echavarren, Antonio M.; Perez, Marta; Castano, Ana M.; Cuerva, Juan M.
Journal of Organic Chemistry, 1994 , vol. 59, # 15 p. 4179 - 4185
反应条件
tetraphenyl stibonium bromide in tetrahydrofuran T=25°C; 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 4 p. 1180 - 1186
反应条件
1: phenyllithium; Mo(CO)6 in diethyl ether T=-60°C; Addition; 2: With boron trifluoride diethyl etherate in diethyl ether T=-60°C; Substitution; 0.25 h; 3: methyl vinyl ketone in diethyl ether T=-60 - 20°C; Addition; Further stages.;
参考文献
Barluenga, Jose; Rodriguez, Felix; Fananas, Francisco J.
Chemistry - A European Journal, 2000 , vol. 6, # 11 p. 1930 - 1937
反应条件
sodium hydroxide in tetrahydrofuran
反应条件
2-(2-hydroxyethyl)-3-methyl-4-benzylthiazolium chloride; triethylamine T=70°C; 12 h;
参考文献
Roth, B. D.; Ortwine, D. F.; Hoefle, M. L.; Stratton, C. D.; Sliskovic, D. R.; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 21 - 31
反应条件
n-Bu4N+CN- in tetrahydrofuran T=-78°C; 1 h;
参考文献
degl'Innocenti, Alessandro; Ricci, Alfredo; Mordini, Alessandro; Reginato, Gianna; Colotta, Vittoria
Gazzetta Chimica Italiana, 1987 , vol. 117, # 11 p. 645 - 648
反应条件
hydrogenchloride in acetic acid T=100°C; 0.166667 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 5 p. 1371 - 1378
反应条件
1: in toluene T=50°C; 48 h; 2: With iron(III) chloride in diethyl ether; toluene 336000 h;
参考文献
Sakurai, Hidehiro; Narasaka, Koichi
Chemistry Letters, 1994 , # 11 p. 2017 - 2020
反应条件
tri-ruthenium(0)dodecacarbonyl in toluene T=140°C; 20 h;
参考文献
Tatamidani, Hiroto; Yokota, Kazuhiko; Kakiuchi, Fumitoshi; Chatani, Naoto
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5615 - 5621