1-苯基-1,4-戊二酮合成路线 (共 177 条)
反应条件
1: 7 percent / Mn(OAc)2, O2 / acetic acid / 39 h / 23 °C 2: 82 percent / KOH / methanol / 30 h / Heating 3: 92 percent / 2 M aq. HCl / acetic acid / 0.33 h / 80 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 5 p. 1371 - 1378
反应条件
1: 82 percent / KOH / methanol / 30 h / Heating 2: 92 percent / 2 M aq. HCl / acetic acid / 0.33 h / 80 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 5 p. 1371 - 1378
反应条件
1: (i) <nBu4N>Br, aq. NaOH, CHCl3, (ii) /BRN= 741886/ 2: Zn, AcOH / ethyl acetate; ethanol View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 39, p. 192 - 196
反应条件
methanol; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine T=80°C; P=3800.26 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
New Journal of Chemistry, , vol. 33, # 5 p. 969 - 971
反应条件
thionyl chloride T=60°C;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 522, p. 269,276
反应条件
hydrogen cation; palladium Yield given. Multistep reaction;
参考文献
Chemistry Letters, , p. 1237 - 1238
反应条件
aluminum oxide in diethyl ether; pentane Ambient temperature; Yield given;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 2.1 p. 202 - 206
Zhurnal Organicheskoi Khimii, , vol. 30, # 2 p. 197 - 200
反应条件
1: KF-18-crown-6 / acetonitrile / 3 h / Heating 2: KMnO4-silica gel / benzene / 2 h / 70 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 11 p. 635 - 636
反应条件
1: methanol 2: KF-18-crown-6 / acetonitrile / 3 h / Heating 3: KMnO4-silica gel / benzene / 2 h / 70 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 11 p. 635 - 636
反应条件
1: 80 percent / toluene / 24 h 2: 80 percent / Na2CO3 / methanol; H2O / 6 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2408 - 2416