((E)-4-氯-2-甲基-丁-2-烯-1-磺酰基)-苯合成路线 （共 7 条）
反应条件
triethyl amine hydrochloride; copper(l) chloride in acetonitrile
T=60°C; 15 h;
参考文献
Min, Jae-Hong; Lee, Jun-Sup; Yang, Jae-Deuk; Koo, Sangho
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7925 - 7927
反应条件
acetic acid; copper(l) chloride; sodium chloride; sulfur dioxide in water; acetone
T=10 - 15°C;
参考文献
Naidan; Smalius
Russian Journal of General Chemistry, 2004 , vol. 74, # 9 p. 1386 - 1388
反应条件
acetic acid; copper(l) chloride; sodium chloride; sulfur dioxide in water; acetone
T=5 - 10°C;
参考文献
Naidan; Smalius
Russian Journal of General Chemistry, 2004 , vol. 74, # 9 p. 1386 - 1388
反应条件
1: NaNO2, conc. HCl / acetic acid
2: 68 percent / SO2, CuCl2.2H2O / acetone; acetic acid
View Scheme
参考文献
Naidan, V. M.; Naidan, G. D.; Drozdova, S. G.; Musienko, V. M.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 2 p. 391 - 395,346 - 349
反应条件
hydrogenchloride; sulfur dioxide; sodium nitrite
Yield given. Multistep reaction;
参考文献
Naidan, V. M.; Naidan, G. D.; Drozdova, S. G.; Musienko, V. M.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 2 p. 391 - 395,346 - 349
反应条件
tin(IV) chloride in 1,2-dichloro-ethane
T=80°C; Friedel-Crafts reaction; 8 h; Product distribution; Further Variations:ReagentsSolventsTemperaturesreaction times;
参考文献
Min, Jae-Hong; Lee, Jun-Sup; Yang, Jae-Deuk; Koo, Sangho
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7925 - 7927
反应条件
1: HCO2H / 2 h / 120 °C
2: aq. HCl / methanol / 25 °C
View Scheme
参考文献
Julia,M. et al.
Bulletin de la Societe Chimique de France, 1976 , p. 519 - 524
