4-(苯甲酰基氨基)苯甲酸合成路线 (共 20 条)
反应条件
potassium hydroxide; water in methanol 3 h;
参考文献
AMOREPACIFIC CORPORATION
Patent: WO2005/19162 A1, 2005 ;
Location in patent: Page/Page column 13-15 ;
反应条件
methanol; sodium hydroxide in tetrahydrofuran T=20°C; 2 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 39 - 44
反应条件
1: benzoic acid With 1-methyl-piperidine; isopropyloxycarbonylchloride in tetrahydrofuran; toluene T=0°C; 0.333333 h; 2: With LiAlHSeH in tetrahydrofuran; toluene T=0 - 5°C; 0.5 h; 3: 4-azidobenzoic acid in tetrahydrofuran; toluene T=25°C;
参考文献
Wu, Xinghua; Hu, Longqin
Journal of Organic Chemistry, 2007 , vol. 72, # 3 p. 765 - 774
反应条件
sodium chloride in water; acetone 0.25 h;
参考文献
Chattopadhyay, Gautam; Chakraborty, Suchandra; Saha, Chandan
Synthetic Communications, 2008 , vol. 38, # 23 p. 4068 - 4075
反应条件
piperidine; N-ethyl-N,N-diisopropylamine in acetonitrile T=25°C; 1 h;
参考文献
Surabhi, Prathima; Wu, Xinghua; Hu, Longqin
Tetrahedron Letters, 2006 , vol. 47, # 27 p. 4609 - 4613
反应条件
potassium permanganate in water 1.5 h; Heating;
参考文献
Lee, Chang Kiu; Ahn, Yu Mi
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3744 - 3747
反应条件
in dimethyl sulfoxide; ethyl acetate T=5 - 20°C; 2 h;
参考文献
Wu, Xinghua; Hu, Longqin
Tetrahedron Letters, 2005 , vol. 46, # 48 p. 8401 - 8405
反应条件
sodium hydrogencarbonate in chloroform; water 1.5 h;
参考文献
Sakakibara, Tohru; Watabe, Yukie; Yamada, Masahide; Sudoh, Rokuro
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 1 p. 247 - 254
反应条件
in N,N-dimethyl-formamide T=80 - 90°C; 4 h;
参考文献
Mashraqui, Sabir Hussain; Shivaji, Jadhav Latika
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 5 p. 927 - 935
反应条件
in N,N-dimethyl-formamide T=70 - 80°C; 3 h;
参考文献
Mashraqui, Sabir H.; Shivaji, Jadhav L.
Journal of Chemical Research - Part S, 2003 , # 3 p. 121 - 123