反应条件
1: 90 percent / SOCl2 / benzene / 5 h / Heating 2: 75 percent / LiBH4 / tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) 20 deg C, 2 h 3: 90 percent / 3 h / Heating 4: 76 percent / 475 °C 5: 79 percent / KOH / ethanol / 8 h / Heating 6: 97 percent / Br2 / diethyl ether / 2 h / -5 °C 7: 66 percent / NaNH2 / tetrahydrofuran; liquid ammonia / 1.) -45 -> -40 deg C, 4 h, 2.) -35 deg C, 1 h View Scheme
参考文献
Zakharkin, L.I.; Churilova, I.M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2414 - 2415
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2635 - 2637
