联苯-2,2-二羧酸二甲酯合成路线 （共 68 条）
反应条件
NiCl2((PPh3)P)2; tetraethylammonium iodide; zinc in tetrahydrofuran
1.) r.t., 5 min, 2.) 67 deg C, 24 h; Yield given;
参考文献
Percec, Virgil; Bae, Jin-Young; Zhao, Mingyang; Hill, Dale H.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 176 - 185
反应条件
bis(acetylacetonato) palladium; 1,10-phenanthroline; potassium carbonate in 1-methyl-pyrrolidin-2-one
T=160°C; 16 h; Inert atmosphereMolecular sieve; chemoselective reaction;
参考文献
Luo, Jiaying; Lu, Youling; Liu, Saiwen; Liu, Jing; Deng, Guo-Jun
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2604 - 2608
反应条件
4-ethyl-1-methyl-4H-[1,2,4]-triazol-1-ium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
T=40°C; TemperatureConcentration;
参考文献
Gundala, Sivaji; Fagan, Claire-Louise; Delany, Eoghan G.; Connon, Stephen J.
Synlett, 2013 , vol. 24, # 10 art. no. ST-2013-R0416-C, p. 1225 - 1228
参考文献
Linstead; Doering
Journal of the American Chemical Society, 1942 , vol. 64, p. 1991,1998
反应条件
9,10-anthracenedicarbonitrile; oxygen in acetonitrile
1.5 h; Ambient temperatureIrradiation;
参考文献
Santamaria, J.; Ouchabane, R.
Tetrahedron, 1986 , vol. 42, # 20 p. 5559 - 5566
反应条件
bis(acetylacetonato) palladium; potassium carbonate; 1,4-di(diphenylphosphino)-butane; copper(l) chloride in 1-methyl-pyrrolidin-2-one
T=160°C; 16 h; Inert atmosphereMolecular sieve; chemoselective reaction;
参考文献
Luo, Jiaying; Lu, Youling; Liu, Saiwen; Liu, Jing; Deng, Guo-Jun
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2604 - 2608
反应条件
hydrogenchloride; methanol; ozone
T=0°C; 34 h; Further byproducts given;
参考文献
Neumeister, Joachim; Griesbaum, Karl
Chemische Berichte, 1984 , vol. 117, # 4 p. 1640 - 1642
反应条件
Chromium (III) chloride in various solvent(s)
Ambient temperature;
参考文献
Ogawa, Yoshihiro; Mori, Mitsuo; Saiga, Akihiro; Takagi, Kentaro
Chemistry Letters, 1996 , # 12 p. 1069 - 1070
反应条件
1: sulfuric acid
2: copper / ethyl acetate / 0.5 h / 205 - 220 °C / Inert atmosphere
View Scheme
参考文献
Sagrera, Gabriel; Bertucci, Ana; Vazquez, Alvaro; Seoane, Gustavo
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 10 p. 3060 - 3073
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; water; 4-ethyl-1-methyl-4H-[1,2,4]-triazol-1-ium iodide / tetrahydrofuran / 20 h / 20 °C
2: magnesium sulfate / tetrahydrofuran / 12 h
View Scheme
参考文献
Gundala, Sivaji; Fagan, Claire-Louise; Delany, Eoghan G.; Connon, Stephen J.
Synlett, 2013 , vol. 24, # 10 art. no. ST-2013-R0416-C, p. 1225 - 1228
