1,5,7-三氮杂双环[4.4.0]癸-5-烯合成路线 （共 17 条）
反应条件
[σ:η1:η5-(OCH2)(Me2NCH2)C2B9H9]Ti-(NMe2) in toluene T=115°C; 240 h;
参考文献
Shen, Hao; Wang, Yang; Xie, Zuowei
Organic Letters, 2011 , vol. 13, # 17 p. 4562 - 4565
反应条件
carbon dioxide in 2-butoxy-ethanol T=60 - 130°C; 6 h;
参考文献
PPG INDUSTRIES OHIO, INC.; ZAWACKY, Steven R.; HICKENBOTH, Charles R.; KARABIN, Richard F.; McCOLLUM, Gregory J.; MORIARITY, Thomas C.
Patent: WO2011/112594 A1, 2011 ;
Location in patent: Page/Page column 18-19 ;
反应条件
1: With hydrogenchloride T=155°C; 2: With sodium methylate in methanol
参考文献
Usachev, Sergei; Gridnev, Alexei
Synthetic Communications, 2011 , vol. 41, # 24 p. 3683 - 3688
反应条件
2-butoxy-ethanol; isopropylamine T=60 - 170°C; 12 h;
参考文献
US2013/289272 A1, ;
Paragraph 0022; 0023 ;
反应条件
2-butoxy-ethanol T=60 - 170°C; 18 h; Reagent/catalystTemperature;
参考文献
US2013/289272 A1, ;
Paragraph 0024; 0025; 0026; 0027; 0030; 0031; 0032; 0033 ;
反应条件
in 2-butoxy-ethanol T=60 - 170°C; 2 h; Inert atmosphere;
参考文献
WO2011/112594 A1, ;
Page/Page column 18 ;
反应条件
in triglyme (triethylene glycol dimethyl ether) T=100 - 230°C; Inert atmosphere; Product distribution / selectivity;
参考文献
US2009/281313 A1, ;
Page/Page column 3 ;
反应条件
1: With hydrogenchloride T=155°C; 2: With sodium methylate in methanol
参考文献
Synthetic Communications, , vol. 41, # 24 p. 3683 - 3688
反应条件
in acetonitrile UV-irradiation at 254 nmInert atmosphere; Quantum yieldKineticsMechanism; TimeConcentration;
参考文献
Journal of the American Chemical Society, , vol. 130, # 26 p. 8130 - 8131
反应条件
in deuterated toluene T=24.84°C; Inert atmosphere; Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 74, # 24 p. 9490 - 9496
