二甲基(甲硫代)锍四氟硼酸盐合成路线 （共 15 条）
反应条件
trimethyl-oxonium tetrafluoroborate in acetonitrile 0.25 h; Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1780 - 1784
参考文献
Helvetica Chimica Acta, , vol. 59, p. 1307 - 1311
反应条件
1.) DMTSF, acetonitrile, 0.5 h 2.) iPr2NEt, acetonitrile, 48 h, room temperature; Yield given. Multistep reaction;
参考文献
O'Malley, Gerard J.; Cava, Michael P.
Tetrahedron Letters, 1985 , vol. 26, # 50 p. 6159 - 6162
反应条件
dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine in nitromethane Ambient temperature;
参考文献
Trost, Barry M.; Shibata, Tohru; Martin, Steven J.
Journal of the American Chemical Society, 1982 , vol. 104, # 11 p. 3228 - 3230
参考文献
Minato,H. et al.
Chemistry Letters, 1975 , p. 701 - 706
反应条件
triethylamine tris-hydrofluoride 1.) 0 deg C, methylene chloride, 20 min, 2.) room temperature, methylene chloride, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Haufe, Guenter; Alvernhe, Gerard; Anker, Daniel; Laurent, Andre; Saluzzo, Christine
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 714 - 719
反应条件
in acetonitrile-D3 N2-atmosphere; slight excess Fe-complex; product mixt. not sepd., detd. by NMR spectroscopy;
参考文献
Treichel; Rublein
Journal of Organometallic Chemistry, 1996 , vol. 512, # 1-2 p. 157 - 164
反应条件
triethylamine tris-hydrofluoride
1.) 0 deg C, methylene chloride, 20 min, 2.) room temperature, methylene chloride, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Haufe, Guenter; Alvernhe, Gerard; Anker, Daniel; Laurent, Andre; Saluzzo, Christine
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 714 - 719
反应条件
in dichloromethane
under N2, 2 equiv ((CH3)2SSCH3)BF4; chromy. (alumina, benzene); evapn.; dissoln. (CH2Cl2); chromy. (alumina, 10 percent CH2Cl2 in Skelly B); evapn.; recrystn.;
参考文献
Treichel, P. M.; Rublein, E. K.
Journal of Organometallic Chemistry, 1992 , vol. 424, # 1 p. 71 - 77
反应条件
dimethyl-disulfide in dichloromethane
T=0°C; 4 h; Title compound not separated from byproducts;
参考文献
Anderson, M.B.; Ranasinghe, M.G.; Palmer, J.T.; Fuchs, P.L.
Journal of Organic Chemistry, 1988 , vol. 53, # 13 p. 3125 - 3127
