1-苯基-1,2-丙二酮合成路线 （共 223 条）
反应条件
titanium(III) chloride in acetic acid
0.666667 h; Ambient temperature;
参考文献
Clerici, Angelo; Porta, Ombretta
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6813 - 6818
反应条件
in acetone
2 h; Irradiation;
参考文献
Dae, Won Cho; Lee, Hyang-Yeol; Sun, Wha Oh; Jung, Hei Choi; Hea, Jung Park; Mariano, Patrick S.; Ung, Chan Yoon
Journal of Organic Chemistry, 2008 , vol. 73, # 12 p. 4539 - 4547
反应条件
titanium(III) chloride in acetic acid
0.666667 h;
参考文献
Clerici, Angelo; Porta, Ombretta
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6813 - 6818
反应条件
1: ethyl bromide With magnesium in diethyl ether
Grignard reaction;
2: 1-phenyl-propane-1,2-dione in diethyl ether
Grignard reaction; Title compound not separated from byproducts;
参考文献
Brunner, Henri; Stoehr, Frank
European Journal of Organic Chemistry, 2000 , # 15 p. 2777 - 2786
反应条件
1: 2) KOH / 1) ethanol, room temp. 1.5 h 2) reflux 5 h
2: 62 percent / 90percent H2O2, maleic anhydride / CH2Cl2 / 48 h / Ambient temperature
3: 15 percent / POCl3 / 1 h / Heating
View Scheme
参考文献
Watahiki, Hiroko; Tsutsui, Mayumi; Akita, Yasuo; Watanabe, Tokuhiro; Kurihara, Teruo
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 465 - 473
反应条件
triethylamine in pentane
参考文献
Gescheidt; Neshchadin; Rist; Borer; Dietliker; Misteli
Physical Chemistry Chemical Physics, 2003 , vol. 5, # 6 p. 1071 - 1077
反应条件
hydrazine hydrate; triethylamine in ethanol
参考文献
Barton, Derek H. R.; Bashiardes, George; Fourrey, Jan-Louis
Tetrahedron, 1988 , vol. 44, # 1 p. 147 - 162
反应条件
in diethyl ether
T=-40°C; 2 h;
参考文献
Saalfrank, Rolf W.; Schierling, Peter; Hafner, Wieland
Chemische Berichte, 1983 , vol. 116, # 10 p. 3482 - 3486
反应条件
1: 53 percent / diethyl ether / 2 h / -40 °C
2: 70 percent / half conc. H2SO4 / CH2Cl2 / 0.25 h / 30 °C
View Scheme
参考文献
Saalfrank, Rolf W.; Schierling, Peter; Hafner, Wieland
Chemische Berichte, 1983 , vol. 116, # 10 p. 3482 - 3486
反应条件
in ethanol
3 h; Heating;
参考文献
Grigor'eva, L. N.; Amitina, S. A.; Volodarskii, L. B.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , p. 1104 - 1108
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 10 p. 1387 - 1392
