苯乙酮乙烷-1,2-二基二硫代缩醛合成路线 （共 34 条）
反应条件
n-butyllithium in diethyl ether T=25°C; 6 h;
参考文献
Wilson, Stephen R.; Georgiadis, Gregory M.; Khatri, Hiralal N.; Bartmess, John E.
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3577 - 3583
反应条件
tert-butylhypochlorite in tetrachloromethane T=20°C; 0.0833333 h;
参考文献
Arote, Nitin D.; Telvekar, Vikas N.; Akamanchi
Synlett, 2005 , # 19 art. no. D25105ST, p. 2935 - 2938
反应条件
n-butyllithium in diethyl ether T=25°C; 6 h;
参考文献
Wilson, Stephen R.; Georgiadis, Gregory M.; Khatri, Hiralal N.; Bartmess, John E.
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3577 - 3583
反应条件
perchloric acid; silica gel
T=25 - 30°C; 5 h;
参考文献
Rudrawar, Santosh; Besra, Ram C.; Chakraborti, Asit K.
Synthesis, 2006 , # 16 p. 2767 - 2771
反应条件
magnesium bromide in diethyl ether
0.5 h; Ambient temperature;
参考文献
Gajare; Shingare; Bandgar
Journal of Chemical Research - Part S, 1998 , # 8 p. 452 - 453
反应条件
tetra-n-butylammonium tribromide in tetrahydrofuran
T=20°C; 0.08 h;
参考文献
Naik, Sarala; Gopinath, Rangam; Goswami, Mousumi; Patel, Bhisma K.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 11 p. 1670 - 1677
反应条件
2,4,4,6-tetrabromo-2,5-cyclohexadien-1-one in chloroform
T=20°C; 0.666667 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza; Zolfigol
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 5 p. 1047 - 1071
参考文献
Uniroyal Inc.; Uniroyal, Ltd.
Patent: US4004018 A1, 1977 ;
反应条件
acetyl chloride in methanol
8 h; Heating;
参考文献
Yu, Haifeng; Liu, Qun; Yin, Yanbing; Fang, Qunxin; Zhang, Jingping; Dong, Dewen
Synlett, 2004 , # 6 p. 999 - 1002
反应条件
silver tetrafluoroborate; PPh3 gold(I) chloro complex in toluene
T=100°C; 20 h;
参考文献
Santos, Laura L.; Ruiz, Violeta R.; Sabater, Maria J.; Corma, Avelino
Tetrahedron, 2008 , vol. 64, # 34 p. 7902 - 7909
