苯乙酮乙烷-1,2-二基二硫代缩醛合成路线 （共 34 条）
反应条件
lithium diisopropyl amide 1.) THF, -15 deg C, 1 h, 2.) THF, a) -10 to -5 deg C, b) RT, 24 h; Yield given. Multistep reaction;
参考文献
Ikehira, Hideyuki; Tanimoto, Shigeo; Oida, Tatsuo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2537 - 2538
反应条件
lithium diisopropyl amide 1.) THF, -15 deg C, 1 h, 2.) THF, a) -10 to -5 deg C, b) RT, 24 h; Yield given. Multistep reaction;
参考文献
Ikehira, Hideyuki; Tanimoto, Shigeo; Oida, Tatsuo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2537 - 2538
反应条件
lithium diisopropyl amide in tetrahydrofuran; cyclohexane 1.) -78 deg C, 20 min; -20 deg C, 30 min, 2.) r.t., overnight;
参考文献
Willmore, Nikolaos D.; Hoic, Diego A.; Katz, Thomas J.
Journal of Organic Chemistry, 1994 , vol. 59, # 7 p. 1889 - 1891
反应条件
1: 85 percent / 85percent 3-Cl-C6H4-COOOH / CH2Cl2 / -20 °C 2: 44 percent / KMnO4 / MgSO4, Me(C8H17)3N(+)Cl(-) / CH2Cl2; H2O / Ambient temperature 3: 60 percent / LDA, HMPT / tetrahydrofuran / 4 h / 0 °C View Scheme
参考文献
Schaumann, Ernst; Ruehter, Gerd
Chemische Berichte, 1988 , vol. 121, p. 1159 - 1164
反应条件
lithium diisopropyl amide 1.) THF, -15 deg C, 1 h, 2.) THF, a) -10 to -5 deg C, b) RT, 24 h; Yield given. Multistep reaction;
参考文献
Ikehira, Hideyuki; Tanimoto, Shigeo; Oida, Tatsuo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2537 - 2538
反应条件
anhydrous magnesium perchlorate; water; methylene green in acetonitrile Irradiation;
参考文献
Epling, Gary A.; Wang, Qingxi
Tetrahedron Letters, 1992 , vol. 33, # 40 p. 5909 - 5912
反应条件
lithium diisopropyl amide 1.) THF, -15 deg C, 1 h, 2.) THF, a) -10 to -5 deg C, b) RT, 24 h; Yield given. Multistep reaction;
参考文献
Ikehira, Hideyuki; Tanimoto, Shigeo; Oida, Tatsuo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2537 - 2538
反应条件
NOBF4; pyridine hydrogenfluoride in dichloromethane 1 h; Ambient temperature;
参考文献
York, Chentao; Prakash, G. K. Surya; Olah, George A.
Tetrahedron, 1996 , vol. 52, # 1 p. 9 - 14
反应条件
pyridine hydrogenfluoride; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in dichloromethane T=20°C;
参考文献
Reddy, V. Prakash; Alleti, Ramesh; Perambuduru, Meher K.; Welz-Biermann, Urs; Buchholz, Herwig; Prakash, G. K. Surya
Chemical Communications, 2005 , # 5 p. 654 - 656
反应条件
n-butyllithium in diethyl ether T=25°C; 6 h;
参考文献
Wilson, Stephen R.; Georgiadis, Gregory M.; Khatri, Hiralal N.; Bartmess, John E.
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3577 - 3583
