2,6,6-三甲基-1-环己烯-1-乙腈合成路线 （共 8 条）
反应条件
hydroxylamine hydrochloride; 1-propanephosphonic acid cyclic anhydride; triethylamine in ethyl acetate; N,N-dimethyl-formamide
T=100°C;
参考文献
Augustine, John Kallikat; Atta, Rajendra Nath; Ramappa, Balakrishna Kolathur; Boodappa, Chandrakantha
Synlett, 2009 , # 20 p. 3378 - 3382
反应条件
BF3·2HOAc in dichloromethane
T=20°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Murai, Akio; Abiko, Atsushi; Kato, Koji; Masamune, Tadashi
Chemistry Letters, 1981 , p. 1125 - 1128
反应条件
1: aq. H2SO4
2: NaBH4
3: PBr3
4: dimethylsulfoxide
View Scheme
参考文献
Bhar, Shanta S.; Ramana
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8935 - 8937
反应条件
1: NaBH4
2: PBr3
3: dimethylsulfoxide
View Scheme
参考文献
Bhar, Shanta S.; Ramana
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8935 - 8937
反应条件
1: PBr3
2: dimethylsulfoxide
View Scheme
参考文献
Bhar, Shanta S.; Ramana
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8935 - 8937
反应条件
1: Bu3SnH / benzene / 3 h / Heating
2: BF3*2AcOH / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Murai, Akio; Abiko, Atsushi; Kato, Koji; Masamune, Tadashi
Chemistry Letters, 1981 , p. 1125 - 1128
反应条件
in dimethyl sulfoxide
参考文献
Bhar, Shanta S.; Ramana
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8935 - 8937
参考文献
Bhar, Shanta S.; Ramana
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8935 - 8937
