1-(4-甲氧基苯基)-3-苯基-丙-1-酮合成路线 (共 53 条)
反应条件
hydrogen in water; acetonitrile T=20°C; P=760.051 Torr; 24 h; Sealed tube;
参考文献
Ding, Boqiang; Zhang, Zhenfeng; Liu, Yangang; Sugiya, Masashi; Imamoto, Tsuneo; Zhang, Wanbin
Organic Letters, 2013 , vol. 15, # 14 p. 3690 - 3693
反应条件
barium hydroxide monohydrate; water; palladium nanoparticles in poly(viologen) T=100°C; 24 h;
参考文献
Yamada, Yoichi M.A.; Uozumi, Yasuhiro
Tetrahedron, 2007 , vol. 63, # 35 p. 8492 - 8498
反应条件
copper ferrite in 1,2-dichloro-ethane T=35 - 38°C; Friedel-Crafts Acylation; 18 h;
参考文献
Parella, Ramarao; Naveen; Kumar, Amit; Babu, Srinivasarao Arulananda
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1738 - 1742
反应条件
tris-(dibenzylideneacetone)dipalladium(0); CsOH; 2,6-bis(N-butyl-N'-methylenebenzimidazolium)-1-bromophenylene dibromide; hydrogen in para-xylene T=125°C; P=760.051 Torr;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 4 p. 896 - 900
反应条件
palladium 10 on activated carbon; sodium carbonate in ethanol; water T=100°C; Heck Reaction; 6 h;
参考文献
Kim, Hyun-Soo; Lee, Sang-Jin; Yoon, Cheol Min
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 1 p. 325 - 327
反应条件
SiClO4; p-trifluoromethylthiobenzoic anhydride; silver perchlorate in dichloromethane 42 h; Ambient temperature;
参考文献
Suzuki; Kitagawa; Mukaiyama
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 12 p. 3729 - 3734
反应条件
1: 3-phenylpropionic acid With N,N'-disuccinimidyl-carbonate; sodium carbonate; tri-cyclo-hexyl-phosphine; Pd(F6-acac)2 in tetrahydrofuran T=60°C; 2: (4-methoxyphenyl)-boronic acid in tetrahydrofuran T=60°C; 20 h; Further stages.;
参考文献
Goossen; Ghosh
Chemical Communications, 2001 , # 20 p. 2084 - 2085
反应条件
pyrrolidine; 1,3-bis-(diphenylphosphino)propane; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=115°C; Heck reaction; 6 h; Molecular sieve;
参考文献
Ruan, Jiwu; Saidi, Ourida; Iggo, Jonathan A.; Xiao, Jianliang
Journal of the American Chemical Society, 2008 , vol. 130, # 32 p. 10510 - 10511
反应条件
bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=100°C; 12 h;
参考文献
Aoki, Satoshi; Fujimura, Tsutomu; Nakamura, Eiichi; Kuwajima, Isao
Journal of the American Chemical Society, 1988 , vol. 110, # 10 p. 3296 - 3298
反应条件
potassium carbonate; [(t-Bu)3PH]BF4; [Rh(C2H4)2Cl]2 in 1,4-dioxane; acetone T=80°C;
参考文献
Chuzel, Olivier; Roesch, Alexander; Genet, Jean-Pierre; Darses, Sylvain
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7800 - 7802