N-甲基-N-(2-甲基苯基)-乙酰胺合成路线 (共 7 条)
反应条件
N-bromosuccinmide in tetrachloromethane 2.5 h; HeatingIrradiation;
参考文献
Collins, David J.; Drygala, Peter F.; Swan, John M.
Australian Journal of Chemistry, 1983 , vol. 36, # 10 p. 2095 - 2110
反应条件
hexamethylenetetramine; hydrobromide; potassium carbonate in benzene
T=8 - 10°C; 0.75 h;
参考文献
Bisarya; Rao
Synthetic Communications, 1992 , vol. 22, # 22 p. 3305 - 3313
参考文献
Monnet; Reverdin; Noelting
Chemische Berichte, 1878 , vol. 11, p. 2278
反应条件
sodium hydride
1.) DMF, 10 min, 2.) DMF, 50 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Collins, David J.; Drygala, Peter F.; Swan, John M.
Australian Journal of Chemistry, 1983 , vol. 36, # 10 p. 2095 - 2110
反应条件
1: hydrochloric acid / 200 - 220 °C / im Autoklaven
View Scheme
参考文献
Monnet; Reverdin; Noelting
Chemische Berichte, 1878 , vol. 11, p. 2278
参考文献
Lander
Journal of the Chemical Society, 1901 , vol. 79, p. 698
Journal of the Chemical Society, 1902 , vol. 81, p. 593
参考文献
Lander
Journal of the Chemical Society, 1901 , vol. 79, p. 698
Journal of the Chemical Society, 1902 , vol. 81, p. 593