3-氯-4-苯基-1,2,5-噻二唑合成路线 （共 8 条）
反应条件
disulfur dichloride in N,N-dimethyl-formamide T=0 - 20°C; 21.3333 h;
参考文献
Nuevolution A/S
Patent: WO2009/152824 A1, 2009 ;
Location in patent: Page/Page column 214-215 ;
反应条件
potassium fluoride; tetrakis(triphenylphosphine) palladium(0) in water; toluene Suzuki cross-coupling reaction; 48 h; Heating;
参考文献
Merschaert, Alain; Gorissen, Hugo J.
Heterocycles, 2003 , vol. 60, # 1 p. 29 - 45
反应条件
potassium fluoride; tetrakis(triphenylphosphine) palladium(0) in water; toluene Suzuki cross-coupling reaction; 26 h; Heating;
参考文献
Merschaert, Alain; Gorissen, Hugo J.
Heterocycles, 2003 , vol. 60, # 1 p. 29 - 45
反应条件
potassium fluoride; tetrakis(triphenylphosphine) palladium(0) in water; toluene Suzuki cross-coupling reaction; Heating;
参考文献
Merschaert, Alain; Gorissen, Hugo J.
Heterocycles, 2003 , vol. 60, # 1 p. 29 - 45
反应条件
trithiazyl trichloride in benzene 87 h; Ambient temperature;
参考文献
Duan, Xiao-Guang; Duan, Xiao-Lan; Rees, Charles W.; Yue, Tai-Yuen
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 17 p. 2597 - 2601
反应条件
disulfur dichloride in N,N-dimethyl-formamide
参考文献
Journal of Organic Chemistry, , vol. 32, p. 2823 - 2829
反应条件
1: 85 percent / disulfur dichloride / CH2Cl2 / 336 h / 20 °C 2: 36 percent / aq. ammonia / acetonitrile / 2 h / 20 - 80 °C View Scheme
参考文献
Molecules, , vol. 10, # 2 p. 346 - 359
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Stille cross-coupling reaction; 24 h; Heating;
参考文献
Merschaert, Alain; Gorissen, Hugo J.
Heterocycles, 2003 , vol. 60, # 1 p. 29 - 45
