N-(4-氯苄基)乙酰胺合成路线 （共 20 条）
反应条件
2-chloro-anthraquinone; oxygen in ethyl acetate T=20°C; 30 h; Irradiation;
参考文献
Itoh, Izuho; Matsusaki, Yoko; Fujiya, Akitoshi; Tada, Norihiro; Miura, Tsuyoshi; Itoh, Akichika
Tetrahedron Letters, 2014 , vol. 55, # 20 p. 3146 - 3148
反应条件
dihydrogen peroxide; bromine in 1,2-dichloro-ethane T=20°C; 3 h;
参考文献
Minisci, Francesco; Punta, Carlo; Recupero, Francesco; Fontana, Francesca; Franco Pedulli, Gian
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2671 - 2676
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate in acetic acid T=100°C; 2 h; Title compound not separated from byproducts.;
参考文献
Minisci, Francesco; Punta, Carlo; Recupero, Francesco; Fontana, Francesca; Franco Pedulli, Gian
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2671 - 2676
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran T=0 - 20°C; Heating / reflux; 2: With hydrogenchloride in water
参考文献
ASTRAZENECA AB; ASTRAZENECA UK LIMITED
Patent: WO2004/294 A1, 2003 ;
Location in patent: Page 30 ;
WO 2004/000294 A1
反应条件
sulfuric acid in water T=60 - 92°C; ΔH(excit.), ΔS(excit.); KineticsMechanismThermodynamic data;
参考文献
Druet, Linda M.; Yates, Keith
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2401 - 2414
反应条件
dihydrogen peroxide; bromine in 1,2-dichloro-ethane T=20°C; 3 h;
参考文献
Chemical Communications, , # 6 p. 523 - 524
反应条件
N-bromosuccinmide in chloroform T=20°C; 18 h;
参考文献
Wang, Guangjun; Li, Zhengwei; Ha, Chengyong; Ding, Ke
Synthetic Communications, 2008 , vol. 38, # 10 p. 1629 - 1637
反应条件
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine in DMF (N,N-dimethyl-formamide)
T=0 - 20°C; 2 h;
参考文献
ASTRAZENECA AB; ASTRAZENECA UK LIMITED
Patent: WO2004/294 A1, 2003 ;
Location in patent: Page 29, 30 ;
WO 2004/000294 A1
反应条件
Montmorillonite KSF; polymer-bound 4-(N-benzyl-N-methylamino)pyridine; hafnium tetrachloride in acetonitrile
24 h; Heating;
参考文献
Shi, Min; Cui, Shi-Cong
Synthetic Communications, 2005 , vol. 35, # 22 p. 2847 - 2858
反应条件
Mg(HSO4)2
T=75°C; 2 h;
参考文献
Salehi; Khodaei; Zolfigol; Keyvan
Synthetic Communications, 2001 , vol. 31, # 13 p. 1947 - 1951
