1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran
T=0°C; 0.0833333 h;
2: 2,2-dimethylpropiophenone in tetrahydrofuran
T=20°C; 23 h;
3: With hydrogenchloride in tetrahydrofuran; water
pH=5;
参考文献
Bert, Katrien; Noel, Timothy; Kimpe, Wim; Goeman, Jan L.; Van Der Eycken, Johan
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 42 p. 8539 - 8550