双-[3-(三乙氧基硅)丙基]-二硫化物合成路线 （共 27 条）
反应条件
1: TESPT With sodium in Solventreg; 140 T=110°C; 0.75 h; 2: octanoic acid chloride in Solventreg; 140 T=45 - 104°C; 1 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
US6777569 B1, ;
Page column 9 ;
反应条件
hydrogen sulfide P=760 Torr; 2.5 h; Irradiation; Yield given;
参考文献
Doklady Chemistry, , vol. 339, # 1-3 p. 205 - 207
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 339, # 1 p. 62 - 64
反应条件
sodium oligosulfide in ethylene glycol dimethyl ether 1 h; Heating; Further byproducts given;
参考文献
Chemistry Letters, , # 4 p. 454 - 455
反应条件
sodium sulfide T=-10 - 120°C; P=2400.24 Torr; 2 - 5.33333 h; Product distribution / selectivity;
参考文献
EP1529782 A1, ;
Page/Page column 9; 10-11; 11; 11-12; ;
反应条件
sodium sulfide T=50 - 102°C; 3 h; Product distribution / selectivity;
参考文献
EP1529782 A1, ;
Page/Page column 10 ;
反应条件
sodium hydrogensulfide in ethanol T=90 - 100°C; 2 - 4 h; Conversion of starting material;
参考文献
EP1538152 A1, ;
Page/Page column 9; 10 ;
反应条件
sodium hydrogensulfide T=90 - 100°C; 2 - 4 h; Conversion of starting material;
参考文献
EP1538152 A1, ;
Page/Page column 10 ;
反应条件
1: 4,4,13,13-tetraethoxy-3,14-dioxa-8,9-dithia-4,13-disilahexadecane With sodium in toluene T=110°C; 0.75 - 1.15 h; 2: octanoic acid chloride in toluene T=45 - 60°C; 1 - 2 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
US6777569 B1, ;
Page column 7-9 ;
反应条件
hydrogen; E105Y/W 5percent Pd in ethanol T=155°C; P=38253.8 Torr; Product distribution / selectivity;
参考文献
Degussa AG
Patent: US2006/252952 A1, 2006 ;
Location in patent: Page/Page column 7-9 ;
