2,3-二溴四氢-2H-吡喃合成路线 （共 9 条）
反应条件
in tetrachloromethane 16 h; Heating;
参考文献
Hoffmann, H. M. R.; Giesel, Kunibert; Lies, Reinhard; Ismail, Zeinhom M.
Synthesis, 1986 , # 7 p. 548 - 551
反应条件
in tetrachloromethane 16 h; Reflux;
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
反应条件
1: tetrachloromethane / 16 h / |Reflux 2: piperidine / 60.5 h / 20 - 30 °C 3: potassium hydroxide / water / 12 h 4: caesium carbonate; hydrogen; C63H78IrNOP(2+)*C32H12BF24(1-) / methanol / 12 h / 60 °C / 4560.31 Torr / |Autoclave View Scheme
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
反应条件
1: CCl4 / 16 h / Heating 2: piperidine / CCl4 / 60 h / Ambient temperature View Scheme
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
反应条件
1: CCl4 / 16 h / Heating 2: piperidine / CCl4 / 60 h / Ambient temperature 3: KOH / H2O / 24 h / Heating View Scheme
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
参考文献
Brandon et al.
Journal of the American Chemical Society, 72 <19050> 2120
反应条件
magnesium ether; Yield given. Multistep reaction;
参考文献
Crombie, Leslie; Wyvill, Robert D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1971 - 1982
反应条件
1: 28 percent / diethyl ether / 12 h / Ambient temperature 2: 66 percent / Na / diethyl ether / 3 h / Heating 3: 94 percent / H2 / 10percent Pd/C / ethyl acetate View Scheme
参考文献
Kovalev, B. G.; Nasser, Fadel' Akhmed; Sorochinskaya, A. M.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 10 p. 1651 - 1653
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 10 p. 1983 - 1986
反应条件
lithium aluminium tetrahydride in diethyl ether Yield given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1971 - 1982
