1-(3,4-二甲氧基苯基)乙醇合成路线 (共 29 条)
反应条件
1: in tetrahydrofuran; methanol T=0°C; 0.0833333 h; 2: With sodium tetrahydroborate in tetrahydrofuran; methanol T=0°C; 6 h;
参考文献
Zhang, Wei; Zhang, Wenxue; Dai, Yisi; Zhu, Haizhen
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1747 - 1750
反应条件
in diethyl ether T=0 - 5°C; Grignard reaction; 2 h;
参考文献
Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 251 - 268
反应条件
water in water T=20 - 24°C; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 106, # 5 p. 1361 - 1372
反应条件
in water T=20 - 24°C; solvolysis;
参考文献
Journal of the American Chemical Society, , vol. 106, # 5 p. 1361 - 1372
反应条件
1: aluminium chloride; CS2 / Erwaermen kurze Zeit auf 50grad, Behandeln des Reaktionsprodukts mit Eis und mit Natronlauge und Destillation 2: sodium; alcohol View Scheme
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 248, p. 143
Chem. Zentralbl., , vol. 80, # I p. 923
反应条件
2: NaBH4 View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 28, p. 453 - 464
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 2142,2144
J. Gen. Chem. USSR (Engl. Transl.), , vol. 27, p. 2200,2202
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 248, p. 143
Chem. Zentralbl., , vol. 80, # I p. 923
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 248, p. 143
Chem. Zentralbl., , vol. 80, # I p. 923
反应条件
morpholinium bisulfate T=20°C; 0.05 h; Neat (no solvent); chemoselective reaction;
参考文献
Hajipour, Abdol R.; Nasresfahani, Zahra
Synthetic Communications, 2012 , vol. 42, # 13 p. 1995 - 2006