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triethylamine; N,N-diethylaniline 6 h; Heating;

triethylamine; N,N-diethylaniline 6 h; Heating;

thionyl chloride

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587154', constants.ctx, '0')">ammonia</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1696894', constants.ctx, '0')">diethyl ether</a> <br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '14402699', constants.ctx, '0')">Cu(BF₄)2</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '8127932', constants.ctx, '0')">sodium bromide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '635680', constants.ctx, '0')">acetone</a> <br />T=15 - 20&deg;C;&nbsp;2.5&nbsp;h;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: sodium nitrite; hydrogen bromide; potassium bromide / -13 &deg;C<br />2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 20 &deg;C<br />3: ammonium hydroxide / water / 20 &deg;C / |Cooling<br /> <br /> &nbsp;