1-甲氧基-4-(苯硫基)-苯合成路线 (共 118 条)
反应条件
hydrogenchloride; phenol in dichloromethane
T=0 - 25°C;
参考文献
Chasar, Dwight W.; Pratt, Timothy M.; Shockcor, J. P.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 183 - 186
反应条件
titanium tetrachloride in dichloromethane
T=20°C; Arylation; 0.5 h;
参考文献
Suwa, Satoshi; Sakamoto, Takeshi; Kikugawa, Yasuo
Chemical and Pharmaceutical Bulletin, 1999 , vol. 47, # 7 p. 980 - 982
反应条件
1: thiophenol With sodium in diethyl ether
Heating;
2: 5-(p-anisyl)thianthrenium bromide in acetonitrile
T=20°C;
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; bis(dibenzylideneacetone)-palladium(0) in acetone; toluene
T=110°C; 6 h; Inert atmosphere;
参考文献
Park, Namjin; Park, Kyungho; Jang, Mihee; Lee, Sunwoo
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4371 - 4378
反应条件
triethylamine in neat (no solvent)
T=90°C; 13 h; Inert atmosphere; chemoselective reaction;
参考文献
Kamal, Ahmed; Srinivasulu, Vunnam; Murty; Shankaraiah, Nagula; Nagesh, Narayana; Reddy, T. Srinivasa; Subba Rao
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 11-12 p. 2297 - 2307
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; NAF in water
T=150°C; 0.333333 h; Microwave irradiation;
参考文献
Velmathi, Sivan; Vijayaraghavan, Reena; Amarendar, Ch.; Pal, Ravindra P.; Vinu, Ajayan
Synlett, 2010 , # 18 p. 2733 - 2736
反应条件
caesium carbonate in dimethyl sulfoxide
T=110°C; 16.5 h; Inert atmosphere; chemoselective reaction;
参考文献
Kamal, Ahmed; Srinivasulu, Vunnam; Murty; Shankaraiah, Nagula; Nagesh, Narayana; Reddy, T. Srinivasa; Subba Rao
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 11-12 p. 2297 - 2307
反应条件
copper(l) iodide; tetrabutyl ammonium fluoride; biphenyl-2-yl-di-tert-butyl-phosphane
T=100°C; 24 h;
参考文献
Luo, Pei-Song; Yu, Ming; Tang, Ri-Yuan; Zhong, Ping; Li, Jin-Heng
Tetrahedron Letters, 2009 , vol. 50, # 9 p. 1066 - 1070
反应条件
1-(2,6-diisopropylphenyl)-3-[2-(mesitylamino)-2-oxoethyl]-1H-imidazol-3-ium bromide; potassium hexamethylsilazane; bis(dibenzylideneacetone)-palladium(0); thiolacetic acid potassium salt in toluene
T=80 - 110°C; 18 h; Inert atmosphere;
参考文献
Byeun, Aleum; Baek, Kyungkyu; Han, Min Su; Lee, Sunwoo
Tetrahedron Letters, 2013 , vol. 54, # 49 p. 6712 - 6715
反应条件
in methanol
T=20 - 25°C; arylthiodediazoniation; dimerization;
参考文献
Barbero, Margherita; Degani, Iacopo; Diulgheroff, Nicola; Dughera, Stefano; Fochi, Rita; Migliaccio, Mara
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5600 - 5608