5,7,4-三甲氧基黄酮合成路线 （共 36 条）
反应条件
N-butyl-N-methylimidazolium heptachlorodialuminate in dichloromethane T=40°C; 4 h;
参考文献
Liu, Tao; Hu, Yongzhou
Synthetic Communications, 2004 , vol. 34, # 17 p. 3209 - 3218
反应条件
boron tribromide in dichloromethane 5 h; Ambient temperature;
参考文献
Zembower, David E.; Zhang, Heping
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9300 - 9305
反应条件
1: 95 percent / dimethyldioxirane / acetone; CH2Cl2 / 8 h 2: 91 percent / BBr3 / CH2Cl2 / 24 h / Heating View Scheme
参考文献
Lee, Yean-Jang; Wu, Tsao-Dong
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 2 p. 201 - 206
反应条件
pyridine hydrochloride T=180 - 190°C; 6 h; Inert atmosphere;
参考文献
Wang, Jin; Zhou, Rong-Guang; Wu, Ting; Yang, Tao; Qin, Qi-Xue; Li, Li; Yang, Bo; Yang, Jian
Journal of Chemical Research, 2012 , vol. 36, # 3 p. 121 - 122
反应条件
N-butyl-N-methylimidazolium heptachlorodialuminate in dichloromethane T=40°C; 4 h;
参考文献
Synthetic Communications, , vol. 34, # 17 p. 3209 - 3218
反应条件
sodium lauryl sulfate in water Irradiationphotocycloaddition in micelles;
参考文献
Hailes; Raphael; Staunton
Tetrahedron Letters, 1993 , vol. 34, # 33 p. 5313 - 5316
反应条件
1: 5,7,4'-trihydroxyflavone With sodium hydride in N,N-dimethyl-formamide
0.166667 h; Cooling with iceInert atmosphere;
2: methyl iodide in N,N-dimethyl-formamide
T=20°C; 20 h; Inert atmosphere;
参考文献
Vins, Petr; Vermachova, Martina; Drasar, Pavel; Del Barrio, Melisa; Jarne, Carmen; Cebolla, Vicente L.; De Cozar, Abel; Zangi, Ronen; Cossio, Fernando P.
Tetrahedron, 2013 , vol. 69, # 48 p. 10361 - 10368
反应条件
sulfuric acid in acetic acid
参考文献
Banerji, Asoke; Goomer, Naresh C.
Synthesis, 1980 , # 11 p. 874 - 875
反应条件
iodine in dimethyl sulfoxide
T=100°C; 4 h;
参考文献
Smith, Jeffrey A.; Maloney, David J.; Hecht, Sidney M.; Lannigan, Deborah A.
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 14 p. 5018 - 5034
反应条件
sodium methylate in methanol
T=0 - 5°C;
参考文献
Bose, Gopal; Mondal, Ejabul; Khan, Abu T; Bordoloi, Manob J.
Tetrahedron Letters, 2001 , vol. 42, # 50 p. 8907 - 8909
