phosphorus tribromide in benzene 20 h; Ambient temperature;
参考文献
Giles, Robin G. F.; Mitchell, Peter R. K.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2147 - 2152
lithium aluminium tetrahydride in diethyl ether
3 h; Heating;
参考文献
Giles, Robin G. F.; Mitchell, Peter R. K.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2147 - 2152
lithium aluminium tetrahydride in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Nicoletti, Teresa M.; Raston, Colin L.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 133 - 138
1: 94 percent / CuCN / dimethylformamide / 6 h / Heating
2: 92 percent / KOH / methanol; H2O / 72 h / Heating
3: 97 percent / LiAlH4 / tetrahydrofuran / 2 h / Ambient temperature
View Scheme
参考文献
Nicoletti, Teresa M.; Raston, Colin L.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 133 - 138
1: 92 percent / KOH / methanol; H2O / 72 h / Heating
2: 97 percent / LiAlH4 / tetrahydrofuran / 2 h / Ambient temperature
View Scheme
参考文献
Nicoletti, Teresa M.; Raston, Colin L.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 133 - 138
1: 97 percent / phosphorus tribromide / benzene / 20 h / Ambient temperature
2: bromine / acetic acid / 5 h / Ambient temperature
View Scheme
参考文献
Giles, Robin G. F.; Mitchell, Peter R. K.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2147 - 2152
