4-硝基喹啉-N-氧化物合成路线 (共 69 条)
反应条件
trifluorormethanesulfonic acid; potassium nitrate; trifluoroacetic acid T=0°C; 25 h;
参考文献
Yokoyama, Akihiro; Ohwada, Tomohiko; Saito, Shinichi; Shudo, Koichi
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 2 p. 279 - 283
反应条件
meta-chloroperoxybenzoic acid in 1,4-dioxane; water T=20°C; Ea, ΔSpercent; Rate constantKineticsThermodynamic data;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 17, # 1 p. 72 - 76
Khimiya Geterotsiklicheskikh Soedinenii, , # 1 p. 89 - 94
反应条件
sulfuric acid; potassium nitrate T=0°C; 10 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 2 p. 279 - 283
反应条件
in water T=25.5°C; concentration, temperature, complex formation, solvent effect, ΔH0=1.62 (+/- 0.13: kcal/mol); ΔS0=11.94 (+/- 0.46: cal/K*mol); in pH=7 buffer solution, I=0.5 with NaCl; Equilibrium constantThermodynamic dataMechanism;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 36, # 10 p. 3753 - 3759
参考文献
Journal of Organic Chemistry, , vol. 18, p. 534,541
Yakugaku Zasshi, , vol. 70, p. 384,387
Chem.Abstr., , p. 2476
参考文献
Journal of Organic Chemistry, , vol. 18, p. 534,541
Yakugaku Zasshi, , vol. 70, p. 384,387
Chem.Abstr., , p. 2476
反应条件
1: 3 - 7 °C 2: phosphorus (V)-chloride; phosphoryl chloride View Scheme
参考文献
Ochiai; Kaneko
Pharmaceutical Bulletin, 1957 , vol. 5, p. 56,60
反应条件
1: phosphorus (III)-bromide; ethyl acetate 2: methanol View Scheme
参考文献
Nakayama
Yakugaku Zasshi, 1951 , vol. 71, p. 1088,1090
Chem.Abstr., 1952 , p. 5046
反应条件
chloroformic acid ethyl ester in 1,2-dichloro-ethane T=40 - 65°C;
参考文献
Veerareddy, Arava; Surendrareddy, Gogireddy; Dubey
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 4 p. 961 - 964
参考文献
Ochiai; Hasegawa
Yakugaku Zasshi, 1945 , vol. 65, p. Ausg. B, S. 58, 59
Chem.Abstr., 1952 , p. 113