in neat (no solvent) byproducts: C, Mg-carbide; in H2 atmosphere start of reaction at gentle heating with deposition of C; at red heat vigorous reaction;;
in neat (no solvent) using a fixed-bed reaction system directly connected to GC-TCD; placing of Mg3(VO4)2 in quartz reactor; injecting of CCl4; heating at 723 K; monitoring by XRD and GC-TCD;
参考文献
Tamai, Tsukasa; Inazu, Koji; Aika, Ken-Ichi
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 8 p. 1565 - 1574