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<b>Multi-step reaction with 2 steps<br /> </b>1: 40 percent / sodium methoxide / methanol / 4 h / -10 &deg;C<br />2: 90 percent / Rh₂(pbf)4 / toluene / 16 h / 40 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: potassium carbonate; potassium iodide / acetone / 12 h / 20 - 60 &deg;C / |Inert atmosphere<br />2: 12 h / 120 &deg;C / |Sealed tube; |Inert atmosphere<br />3: iodine / neat (no solvent) / 0.2 h / 20 &deg;C<br /> <br /> &nbsp;