1,1-二氯-4-甲基-1,3-戊二烯合成路线 （共 44 条）
反应条件
1: 20 percent / Cu2O, CuCl, dibutylamine / 1 h / 100 - 110 °C
2: 87 percent / Zn/Cu / methanol
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参考文献
Badanyan; Stepanyan; Mikaelyan; Ovivyan; Panosyan
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 1 p. 34 - 41
反应条件
1: 20 percent / Cu2O, CuCl, dibutylamine / 1 h / 100 - 110 °C
2: 87 percent / Zn/Cu / methanol
3: 80 percent / HCl / 4 h / Ambient temperature
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参考文献
Badanyan; Stepanyan; Mikaelyan; Ovivyan; Panosyan
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 1 p. 34 - 41
反应条件
sodium acetate in dichloromethane; water
参考文献
A/S Cheminova
Patent: US4229353 A1, 1980 ;
反应条件
1: copper-powder / Erhitzen des Reaktionsprodukts mit Essigsaeure und wss. HCl
2: SOCl2; hexane / Behandeln des Reaktionsprodukts mit (+-)-2-Allyl-4-hydroxy-3-methyl-cyclopent-2-enon in Benzol und Pyridin
View Scheme
参考文献
Farkas et al.
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 2230,2235
