反应条件
1: 2-methyl-5-methylpyridine With N,N,N',N,-tetramethylethylenediamine; lithium diisopropyl amide in tetrahydrofuran
T=-78°C; 1 h;
2: chloroformic acid ethyl ester in tetrahydrofuran
T=-78 - 20°C; 12 h;
参考文献
Jiang, Jinlong; DeVita, Robert J.; Goulet, Mark T.; Wyvratt, Matthew J.; Lo, Jane-L.; Ren, Ning; Yudkovitz, Joel B.; Cui, Jisong; Yang, Yi T.; Cheng, Kang; Rohrer, Susan P.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 7 p. 1795 - 1798
