2,5-吡啶二甲酸二乙酯合成路线 (共 18 条)
参考文献
Bisel, Philippe; Gies, Jean Pierre; Schlewer, Gilbert; Wermuth, Camille G.
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 24 p. 3025 - 3028
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; sodium acetate; palladium diacetate T=135°C; Carboxylation; P=11250.9 Torr; 1 h;
参考文献
Heterocycles, , vol. 51, # 11 p. 2589 - 2602
参考文献
Arhiv za Kemiju, , vol. 18, p. 3,6
Chem.Abstr., , p. 3398
Kobunshi Kagaku, , vol. 15, p. 839,844
Chem.Abstr., , p. 22636
反应条件
2 h; Heating; Yield given;
参考文献
Synthesis, , # 4 p. 597 - 602
反应条件
Title compound not separated from byproducts;
参考文献
Schlecker, Wolfgang; Huth, Andreas; Otow, Eckhard
Journal of Organic Chemistry, 1995 , vol. 60, # 26 p. 8414 - 8416
反应条件
sodium tetrahydroborate; CaCl2 in ethanol; water
参考文献
SRI International
Patent: US4526787 A1, 1985 ;
反应条件
sodium tetrahydroborate; calcium chloride in ethanol 16 h; Ambient temperature;
参考文献
Woersdoerfer, Udo; Voegtle, Fritz; Nieger, Martin; Waletzke, Mirko; Grimme, Stefan; Glorius, Frank; Pfaltz, Andreas
Synthesis, 1999 , # 4 p. 597 - 602
反应条件
ethanol; sodium ethanolate T=110°C; beim anschliessenden Erhitzen mit wss. Salzsaeure;
参考文献
Prostenik; Filipovic
Arhiv za Kemiju, 1946 , vol. 18, p. 3,6
Chem.Abstr., 1948 , p. 3398
反应条件
1: NaBH4; CaCl2 2: 94 percent / CCl4; nBu3P / 0.25 h View Scheme
参考文献
Ojaimi, Maya El; Habermeyer, Benoit; Gros, Claude P.; Barbe, Jean-Michel
Journal of Porphyrins and Phthalocyanines, 2010 , vol. 14, # 6 p. 469 - 480
反应条件
sodium tetrahydroborate; calcium chloride in methanol
参考文献
Bisel, Philippe; Gies, Jean Pierre; Schlewer, Gilbert; Wermuth, Camille G.
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 24 p. 3025 - 3028