1-甲基-9H-芴-9-酮合成路线 （共 38 条）
反应条件
phosphorus; hydrogen iodide in propionic acid 24 h; Heating;
参考文献
Evonik Degussa GmbH
Patent: EP1894938 A1, 2008 ;
Location in patent: Page/Page column 34-35 ;
参考文献
Lothrop; Goodwin
Journal of the American Chemical Society, 1943 , vol. 65, p. 363,365
反应条件
potassium permanganate
参考文献
Kruber; Raeithel
Chemische Berichte, 1954 , vol. 87, p. 1469,1475
反应条件
1: diethyl ether 2: H2 / Pd-C View Scheme
参考文献
McDowell,B.L. et al.
Journal of the American Chemical Society, 1962 , vol. 84, p. 3531 - 3538
反应条件
CsO2CCMe3; [Pd(P{(C6H11)3})2] in N,N-dimethyl-formamide
T=110°C; Carbonylation; cyclization; P=760.051 Torr; 7 h;
参考文献
Campo, Marino A.; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 16 p. 5616 - 5620
反应条件
methanesulfonic acid
T=50 - 60°C;
参考文献
Tilly, David; Samanta, Subhendu S.; Castanet, Anne-Sophie; De, Asish; Mortier, Jacques
European Journal of Organic Chemistry, 2006 , # 1 p. 174 - 182
反应条件
1: With palladium diacetate; copper(II) bis(trifluoromethanesulfonate) in 1,4-dioxane
T=90°C; Molecular sieve;
2: With trifluorormethanesulfonic acid in 1,4-dioxane
T=90°C;
3: With hydrogenchloride; water in 1,4-dioxane
参考文献
Sun, Chang-Liang; Liu, Na; Li, Bi-Jie; Yu, Da-Gang; Wang, Yang; Shi, Zhang-Jie
Organic Letters, 2010 , vol. 12, # 1 p. 184 - 187
反应条件
(i) aq. HCl, EtOH, (ii) NaNO2, (iii) (heating); Multistep reaction;
参考文献
Gosnay,I. et al.
Israel Journal of Chemistry, 1972 , vol. 10, p. 423 - 437
反应条件
tert.-butylhydroperoxide; biscyclopentadienyliron(II) in decane; acetonitrile
T=20 - 90°C; 24 h;
参考文献
Wertz, Sebastian; Leifert, Dirk; Studer, Armido
Organic Letters, 2013 , vol. 15, # 4 p. 928 - 931
反应条件
dipotassium peroxodisulfate; silver(I) acetate in acetonitrile-D3
T=130°C; Pschorr reaction; 1 h; Microwave irradiation;
参考文献
Seo, Sangwon; Slater, Mark; Greaney, Michael F.
Organic Letters, 2012 , vol. 14, # 10 p. 2650 - 2653
