2,2-二甲基-4-戊烯醛合成路线 （共 65 条）
反应条件
aluminum oxide; palladium/alumina Hydrogenation;
参考文献
Opitz,G.; Mildenberger,H.
Angewandte Chemie, 1960 , vol. 72, p. 169
反应条件
(PPh3)2Co(dppe) in acetonitrile; benzene T=70°C; 3 h; Yield given;
参考文献
Vinogradov, M. G.; Tuzikov, A. B.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 11.2 p. 2353 - 2356
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 11 p. 2565 - 2568
反应条件
1: diethyl ether 2: H2 / Pd-C / methanol View Scheme
参考文献
Dillenberger,Z. et al.
Helvetica Chimica Acta, 1978 , vol. 61, p. 1856 - 1902
反应条件
hydroxylamine hydrochloride; 1-propanephosphonic acid cyclic anhydride; triethylamine in ethyl acetate; N,N-dimethyl-formamide T=100°C;
参考文献
Augustine, John Kallikat; Atta, Rajendra Nath; Ramappa, Balakrishna Kolathur; Boodappa, Chandrakantha
Synlett, 2009 , # 20 p. 3378 - 3382
反应条件
amalgamated magnesium in diethyl ether
参考文献
Stevens,R.V. et al.
Journal of the American Chemical Society, 1971 , vol. 93, p. 6629 - 6637
参考文献
Wang, Lin; Arthur, Samuel David; McCord, Elizabeth Forrester; Wang, Yueli; Morken, Peter Arnold; Johnson, Lynda Kaye
Patent: US2003/212225 A1, 2003 ;
反应条件
(i) NaNH2, liq. NH3, (ii) /BRN= 1699095/; Multistep reaction;
参考文献
Dillenberger,Z. et al.
Helvetica Chimica Acta, 1978 , vol. 61, p. 1856 - 1902
反应条件
1: 98 percent / Ti(OEt)4 / tetrahydrofuran / 16 h / 20 °C 2: 100 percent / CH2Cl2 / 0 - 20 °C 3: 89 percent / aq. NaOH View Scheme
参考文献
Dondas, H. Ali; De Kimpe, Norbert
Tetrahedron Letters, 2005 , vol. 46, # 24 p. 4179 - 4182
反应条件
1: PdCl2; CuCl; O2 / dimethylformamide; H2O / 72 h 2: KOH / tetrahydrofuran; diethyl ether / 96 h / Heating View Scheme
参考文献
Magnus, P. D.; Nobbs, M. S.
Synthetic Communications, 1980 , vol. 10, # 4 p. 273 - 278
反应条件
aluminum isopropoxide in water
参考文献
Kuraray Company Ltd.
Patent: US5087762 A1, 1992 ;
