1,3-二苯基异苯并呋喃合成路线 （共 125 条）
反应条件
PPA T=110°C; 0.166667 h;
参考文献
Oida, Tatsuo; Tanimoto, Shigeo; Sugimoto, Toyonari; Okano, Masaya
Synthesis, 1980 , # 2 p. 131 - 133
反应条件
1: air; ethanol 2: ethanolic KOH View Scheme
参考文献
Journal of the American Chemical Society, , vol. 70, p. 2069,2072
反应条件
in benzene T=130°C; 27 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 2 p. 395 - 400
反应条件
potassium tert-butylate in tert-butyl alcohol 17 h; Heating; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 45, # 20 p. 3982 - 3986
反应条件
1.1: n-butyllithium / tetrahydrofuran / -78 - 20 °C 2.1: manganese(IV) oxide / dichloromethane / 0 - 20 °C 2.2: 50 °C 3.1: iodine / methanol / 5 h / 20 °C 4.1: tetrakis(triphenylphosphine) palladium(0); lithium chloride / N,N-dimethyl-formamide / 100 °C 5.1: Grubb's 2nd generation catalyst / dichloromethane / Reflux 6.1: palladium 10 on activated carbon; oxygen / toluene / Molecular sieve; Reflux View Scheme
参考文献
Tetrahedron, , vol. 67, # 52 p. 10147 - 10155
反应条件
1.1: toluene-4-sulfonic acid / dichloromethane / 20 °C 2.1: n-butyllithium / tetrahydrofuran / -78 - 20 °C 3.1: manganese(IV) oxide / dichloromethane / 0 - 20 °C 3.2: 50 °C 4.1: iodine / methanol / 5 h / 20 °C 5.1: tetrakis(triphenylphosphine) palladium(0); lithium chloride / N,N-dimethyl-formamide / 100 °C 6.1: Grubb's 2nd generation catalyst / dichloromethane / Reflux 7.1: palladium 10 on activated carbon; oxygen / toluene / Molecular sieve; Reflux View Scheme
参考文献
Tetrahedron, , vol. 67, # 52 p. 10147 - 10155
反应条件
in benzene T=80°C; 11 h; Yield given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 2 p. 395 - 400
反应条件
1: tetrakis(triphenylphosphine) palladium(0); lithium chloride / N,N-dimethyl-formamide / 100 °C 2: Grubb's 2nd generation catalyst / dichloromethane / Reflux 3: palladium 10 on activated carbon; oxygen / toluene / Molecular sieve; Reflux View Scheme
参考文献
Tetrahedron, , vol. 67, # 52 p. 10147 - 10155
反应条件
1: Grubb's 2nd generation catalyst / dichloromethane / Reflux 2: palladium 10 on activated carbon; oxygen / toluene / Molecular sieve; Reflux View Scheme
参考文献
Tetrahedron, , vol. 67, # 52 p. 10147 - 10155
反应条件
1: iodine / dichloromethane / 24 h / 20 °C 2: tetrakis(triphenylphosphine) palladium(0); lithium chloride / N,N-dimethyl-formamide / 100 °C 3: Grubb's 2nd generation catalyst / dichloromethane / Reflux 4: palladium 10 on activated carbon; oxygen / toluene / Molecular sieve; Reflux View Scheme
参考文献
Tetrahedron, , vol. 67, # 52 p. 10147 - 10155
