1,3-二苯基异苯并呋喃合成路线 (共 125 条)
反应条件
4 Angstroem MS; [ReBr(CO)3(thf)]2 in toluene T=115°C; 24 h;
参考文献
Kuninobu, Yoichiro; Nishina, Yuta; Takai, Kazuhiko
Tetrahedron, 2007 , vol. 63, # 35 p. 8463 - 8468
反应条件
4 Angstroem MS; [ReBr(CO)3(thf)]2 in toluene T=115°C; 24 h;
参考文献
Kuninobu, Yoichiro; Nishina, Yuta; Nakagawa, Chie; Takai, Kazuhiko
Journal of the American Chemical Society, 2006 , vol. 128, # 38 p. 12376 - 12377
反应条件
1: in tetrahydrofuran T=-40 - 0°C; 1 h; 2: With trifluoroacetic acid in tetrahydrofuran T=25°C; 1.5 h;
参考文献
Hamura, Toshiyuki; Nakayama, Ryosuke
Chemistry Letters, 2013 , vol. 42, # 9 p. 1013 - 1015
反应条件
triethylsilane; scandium tris(trifluoromethanesulfonate) in chloroform-d1 T=135°C; 0.166667 h; Inert atmosphere;
参考文献
Nishina, Yuta; Kida, Tatsuya; Ureshino, Tomonari
Organic Letters, 2011 , vol. 13, # 15 p. 3960 - 3963
反应条件
tris (α-naphthyl)phosphine; potassium carbonate; palladium dichloride in tetrahydrofuran T=65°C; 24 h; Inert atmosphere;
参考文献
Jacq, Jerome; Bessieres, Bernard; Einhorn, Cathy; Einhorn, Jacques
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 21 p. 4927 - 4933
反应条件
1: benzyl alcohol With [{(η5-C5Me5)IrCl}2(μ-Cl)2]; (E)-3-methylpent-3-en-2-one; potassium carbonate in toluene T=150°C; 18 h; 2: triethylsilane; benzophenone anil With [ReBr(CO)3(thf)]2 in toluene T=115°C; 24 h; Molecular sieve;
参考文献
Kuninobu, Yoichiro; Asanoma, Daisuke; Takai, Kazuhiko
Synlett, 2010 , # 19 p. 2883 - 2886
反应条件
in tetrahydrofuran T=20°C;
参考文献
Benderradji, Farah; Nechab, Malek; Einhorn, Cathy; Einhorn, Jacques
Synlett, 2006 , # 13 p. 2035 - 2038
反应条件
1: T=-40 - 0°C; 2: With trifluoroacetic acid
参考文献
Hamura, Toshiyuki; Nakayama, Ryosuke
Chemistry Letters, 2013 , vol. 42, # 9 p. 1013 - 1015
反应条件
PPA T=110°C; 0.166667 h;
参考文献
Oida, Tatsuo; Tanimoto, Shigeo; Sugimoto, Toyonari; Okano, Masaya
Synthesis, 1980 , # 2 p. 131 - 133
反应条件
palladium 10 on activated carbon; oxygen in toluene Molecular sieveReflux;
参考文献
Yang, Fan; Jin, Tienan; Bao, Ming; Yamamoto, Yoshinori
Tetrahedron, 2011 , vol. 67, # 52 p. 10147 - 10155