in tetrahydrofuran under N2, addn. of Li-compd. in THF over 30 min at 0°C to Me3SnCl in THF, stirred for 18 h; removal of solvent, residue washed with water, extd. (ether), recrystd. (hexane);
参考文献
Dallaire; Brook; Bain; Frampton; Britten
Canadian Journal of Chemistry, 1993 , vol. 71, # 10 p. 1676 - 1683
1: tetrahydrofuran / 48 h / Heating 2: CHCl3 / 4 h / Heating View Scheme
参考文献
Boyer-Elma, Karine; Carre, Francis H.; Corriu, Robert J.-P.; Douglas, William E.
Journal of the Chemical Society, Chemical Communications, 1995 , # 7 p. 725 - 726