N-(2-苯基乙基)-苯乙酰胺合成路线 (共 25 条)
反应条件
in neat (no solvent) T=150°C; 0.5 h; Microwave irradiation; TemperatureTime;
参考文献
Gruen, Alajos; Milen, Matyas; Foeldesi, Tamas; Abranyi-Balogh, Peter; Drahos, Laszlo; Keglevich, Gyoergy
Synthetic Communications, 2013 , vol. 43, # 11 p. 1491 - 1498
反应条件
sodium hydroxide in water T=0°C; 1 h;
参考文献
Nagubandi, Sreeramulu; Fodor, G.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1457 - 1463
反应条件
in dimethyl sulfoxide 15 h; Product distribution / selectivity;
参考文献
The Regents of the University of California
Patent: US2007/60773 A1, 2007 ;
Location in patent: Page/Page column 8-10 ;
反应条件
in water; tert-butyl alcohol T=40°C; 15 h;
参考文献
Arora, Jasbir Singh; Kaur, Navneet; Phanstiel IV, Otto
Journal of Organic Chemistry, 2008 , vol. 73, # 16 p. 6182 - 6186
反应条件
triethylamine in chloroform T=0°C;
参考文献
Martin, Ned H.; Jefford, Charles W.
Helvetica Chimica Acta, 1982 , vol. 65, # 3 p. 762 - 774
反应条件
in dimethyl sulfoxide T=40°C; 15 h;
参考文献
Bode, Jeffrey W.; Fox, Ryan M.; Baucom, Kyle D.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 8 p. 1248 - 1252
反应条件
1: oxalyl chloride; DMF / CH2Cl2 / 12 h 2: Et3N; 4-N,N-dimethylaminopyridine / CH2Cl2 / 48 h / 0 - 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 24 p. 8686 - 8696
反应条件
in methanol T=35 - 40°C; 18 h; Inert atmosphere;
参考文献
Sanki, Aditya K.; Talan, Rommel S.; Sucheck, Steven J.
Journal of Organic Chemistry, 2009 , vol. 74, # 5 p. 1886 - 1896
反应条件
in water; tert-butyl alcohol T=20°C; 0.5 h; chemoselective reaction;
参考文献
Dumas, Aaron M.; Molander, Gary A.; Bode, Jeffrey W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5683 - 5686
反应条件
titanium tetrachloride in dichloromethane T=20°C;
参考文献
Tetrahedron, , vol. 63, # 36 p. 9007 - 9015