1-甲基-4-(仲-丁硫基)苯合成路线 (共 5 条)
反应条件
[(t-Bu)2P(OH)]2PdCl2 ; sodium t-butanolate in dimethyl sulfoxide
T=110°C;
参考文献
Li; Zheng; Noonan
Journal of Organic Chemistry, 2001 , vol. 66, # 25 p. 8677 - 8681
参考文献
Taylor
Journal of the American Chemical Society, 1936 , vol. 58, p. 2649,2650
参考文献
Bordwell; Landis
Journal of the American Chemical Society, 1957 , vol. 79, p. 1593,1596
反应条件
sodium carbonate
1) DMF, 10 min, heating, 2) 30 min, reflux; Yield given. Multistep reaction;
参考文献
Bergman, Jan; Norrby, Per-Ola; Sand, Peter
Tetrahedron, 1990 , vol. 46, # 17 p. 6113 - 6124
反应条件
diisopropylamine
1.) Et2O, 0 deg C, 1 h, 2.) Et2O, RT, 1 h; Yield given. Multistep reaction;
参考文献
Kobayashi, Kazuhiro; Yokota, Kouichi; Akamatsu, Hideki; Morikawa, Osamu; Konishi, Hisatoshi
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 2 p. 441 - 443