N,N-二乙基-1-萘羧酰胺合成路线 （共 22 条）
反应条件
Schwartz's reagent in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Leighty, Matthew W.; Spletstoser, Jared T.; Georg, Gunda I.
Organic Syntheses, 2012 , vol. 88, p. 427 - 437
反应条件
1: 1.) TMEDA, triphenylmethyl chloride, sec-BuLi, 2.) p-toluenesulfonic acid / 1.) ether, cyclohexane, -78 deg C, 1 h, 2.) benzene, reflux 2: 54 percent / HI, P (red) / acetic acid / 56 h / Heating View Scheme
参考文献
Harvey, Ronald G.; Cortez, Cecilia; Jacobs, Stephen A.
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2120 - 2125
反应条件
1: 1.) TMEDA, triphenylmethyl chloride, sec-BuLi / 1.) ether, cyclohexane, -78 deg C, 1 h, 2.) a) -78 deg C, 1 h, b) room temp., 3 h 2: 93 percent / Zn, pyridine, 10percent KOH / Heating; overnight 3: 89 percent / ZnCl2 / acetic acid / 2 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 11 p. 2120 - 2125
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane 1.) -78 deg C, 30 min, 2.) -78 deg C, 30 min;
参考文献
Bowles, Peter; Clayden, Jonathan; Helliwell, Madeleine; McCarthy, Catherine; Tomkinson, Matthew; Westlund, Neil
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 17 p. 2607 - 2616
反应条件
1: 1.) TMEDA, triphenylmethyl chloride, sec-BuLi / 1.) ether, cyclohexane, -78 deg C, 1 h, 2.) a) -78 deg C, 1 h, b) room temp., 3 h 2: 93 percent / Zn, pyridine, 10percent KOH / Heating; overnight 3: 89 percent / ZnCl2 / acetic acid / 2 h / Heating 4: 85 percent / activated Zn dust, NaOH / H2O; dioxane / Heating View Scheme
参考文献
Harvey, Ronald G.; Cortez, Cecilia; Jacobs, Stephen A.
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2120 - 2125
反应条件
potassium phosphate; Pd((imidazolium)acetonaphthene)(allyl)Cl in toluene
T=90°C; P=760.051 Torr; 19 h; Schlenk technique;
参考文献
Fang, Weiwei; Deng, Qinyue; Xu, Mizhi; Tu, Tao
Organic Letters, 2013 , vol. 15, # 14 p. 3678 - 3681
反应条件
triethylamine; Pd-bis(1-methylbenzothiazole-2-carbene) in N,N-dimethyl acetamide
T=130°C; 7 h;
参考文献
Calo, Vincenzo; Giannoccaro, Potenzo; Nacci, Angelo; Monopoli, Antonio
Journal of Organometalic Chemistry, 2002 , vol. 645, # 1-2 p. 152 - 157
反应条件
potassium phosphate; PdClMe(1,5-cyclooctadiene) in 1,4-dioxane
T=100°C; P=7600 Torr; 15 h;
参考文献
Tsukada, Naofumi; Ohba, Yoichi; Inoue, Yoshio
Journal of Organometallic Chemistry, 2003 , vol. 687, # 2 p. 436 - 443
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water
T=90°C; 24 h;
参考文献
Liu, Zhaojun; Zhang, Jie; Chen, Shulin; Shi, Erbo; Xu, Yuan; Wan, Xiaobing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 13 p. 3231 - 3235
参考文献
Alexander,B.H. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 626 - 632
