1-氯-3-甲烷磺酰基-丙烷合成路线 （共 3 条）
反应条件
1: in N,N-dimethyl-formamide
T=20 - 70°C;
2: With 3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C; Overall yield = 0.3 g;
参考文献
CALITHERA BIOSCIENCES INC.; LI, Jim; CHEN, Lijing; GOYAL, Bindu; LAIDIG, Guy; STANTON, Timothy, Friend; SJOGREN, Eric, Brian
Patent: WO2013/78123 A1, 2013 ;
Location in patent: Page/Page column 128 ;
WO 2013/078123 A1
反应条件
2,6-di-tert-butyl-pyridine; nBu4NPF6 in water; acetonitrile
12 h; electrolysis at controlled potential;
参考文献
Aced, Ahmed; Anklam, Elke; Asmus, Klaus-Dieter; Pohl, Klaus; Glass, Richard S.; et al.
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 48, # 1-4 p. 53 - 62
反应条件
2,6-di-tert-butyl-pyridine; nBu4NPF6 in water; acetonitrile
electrolysis at controlled potential;
参考文献
Aced, Ahmed; Anklam, Elke; Asmus, Klaus-Dieter; Pohl, Klaus; Glass, Richard S.; et al.
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 48, # 1-4 p. 53 - 62
