5-硝基-2-甲氧基吡啶合成路线 (共 48 条)
反应条件
sodium T=70°C; 24 h; Heating;
参考文献
Kamogawa, Hiroyoshi; Kasai, Tsuneharu
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 69 - 78
反应条件
sulfuric acid; nitric acid in sulfuric acid T=90 - 100°C; 3 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, # 1 p. 145 - 147
反应条件
methanol; water; sodium sulfite
参考文献
Journal of the American Chemical Society, , vol. 64, p. 1695,1698
反应条件
1: methanol With N-benzyl-trimethylammonium hydroxide 0.166667 h; Neat (no solvent); 2: 2-iodo-5-nitropyridine T=20°C; 0.0833333 h; Neat (no solvent);
参考文献
Meshram; Goud, P. Ramesh; Reddy, B. Chennakesava; Kumar, D. Aravind
Synthetic Communications, 2010 , vol. 40, # 14 p. 2122 - 2129
反应条件
sulfuric acid; nitric acid T=75°C; 1.5 h;
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 6 p. 733 - 746
反应条件
sodium hydride T=23°C; 16 h;
参考文献
Bakke, Jan M.; Sletvold, Ingrid
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 15 p. 2710 - 2715
反应条件
1: aq. KMnO4 / 10 h / 20 °C 2: 115 mg / 20 h / 65 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 15 p. 2710 - 2715
参考文献
Bakke, Jan M.; Sletvold, Ingrid
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 15 p. 2710 - 2715
反应条件
methanol; sodium methylate
参考文献
Justus Liebigs Annalen der Chemie, , vol. 484, p. 52,62
反应条件
1: aqueous hydrofluoric acid / Behandeln der Reaktionsloesung mit Natriumnitrit View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 31, p. 1020,1024