(2R,3R,4S,5S)-1,1-双(乙基磺酰基)己烷-2,3,4,5-四醇合成路线 （共 7 条）
反应条件
1,4-dioxane; peroxypropionic acid; water
参考文献
Justus Liebigs Annalen der Chemie, , vol. 628, p. 186,189
反应条件
1: hydrogen chloride; dioxane 2: dioxane; peroxypropionic acid; water View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 628, p. 186,189
参考文献
Justus Liebigs Annalen der Chemie, , vol. 628, p. 186,189
反应条件
bei Behandeln des Reaktionsprodukts mit Methanol;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 628, p. 186,189
参考文献
Shiratori Pharmaceutical Co., Ltd.; DAIICHI SUNTORY PHARMA CO., LTD.
Patent: US2006/142573 A1, 2006 ;
Location in patent: Page/Page column 5 ;
反应条件
1.1: ammonium hydroxide / water / 14 h / 22 °C / pH 9 - 10 / yellow light 2.1: methanol / 1 h / 20 °C / yellow light 3.1: pyridine / methanol / 0 - 20 °C / yellow light 4.1: sodium acetate; pyridine; sodium dithionite / water; methanol / 20 h / 35 - 40 °C / Inert atmosphere; sealed vessel; yellow light 4.3: 1 h / 50 °C View Scheme
参考文献
KANEKA CORPORATION
Patent: US2011/218339 A1, 2011 ;
反应条件
Yield given. Multistep reaction;
参考文献
Schircks, Bernhard; Bieri, Jost H.; Viscontini, Max
Helvetica Chimica Acta, 1985 , vol. 68, p. 1639 - 1643
